Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Peroxide → Chalcone epoxide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Peroxide | HCID 784 | — |
| 반응물 | Cinnamoylbenzene | HCID 7189 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Chalcone epoxide | HCID 92219 | 22% |
반응 단계
1.040 g (5 mmol) of chalcone was dissolved in 15 ml of ethanol and to the solution was added 2 ml of 25% hydrogen peroxide and 2 ml of an aqueous solution of 1 M sodium carbonate. The precipitate which was formed after stirring for 3 h was isolated and recrystallized from DMSO-water to give 250 mg (22%) of chalcone epoxide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06603046B1 |
| 출처 데이터셋 | uspto-grants-2003_08 |
| ORD ID | ord-237e2fdfe3354990828bfac22728a36b |
| 출처 메모 | uspto-grants-2003_08 |