Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propanoic acid, 2,2,3,3,3-pentafluoro-, methyl ester → Sodium pentafluoropropionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propanoic acid, 2,2,3,3,3-pentafluoro-, methyl ester | HCID 9783 | — |
| 반응물 | Sodium trimethylsilanolate | HCID 23672319 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Sodium pentafluoropropionate | HCID 2733305 | 92% |
반응 단계
The procedure of Example 1 was followed using methyl perfluoropropionate (3 mL, 23.4 mmol), sodium trimethylsilanolate (2.63 g, 23.4 mmol), dry methylene chloride (100 mL), and a 1 h reaction time. Sodium perfluoropropionate (4.0 g, 92% yield) was obtained as a white solid: 1H NMR (D2O) δ -82.4 (t, J=2 Hz, CF3, 3F), -120.1 ppm (q, J=2 Hz, CF2, 2F).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04723016 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-f50e1f0a36124d9191e96386a1984340 |
| 출처 메모 | uspto-grants-1988_02 |