참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,4-Dioxane | HCID 31275 | — |
| 반응물 | 6-Chloroquinaldine | HCID 135965 | — |
| 생성물 | 6-Chloroquinoline-2-carbaldehyde | HCID 271283 | — |
반응 단계
A suspension of 6-chloro-2-methyl-quinoline (355 mg) and SeO2 (233 mg) in 1,4-dioxane (3 mL) was heated at 80° C. for 16 h. The resulting black mixture was filtered through diatomaceous earth. Concentration of the filtrate gave the title compound as a yellow powder (324 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08530476B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_09 |
|---|
| ORD ID | ord-2952c511f0834aa6ab9efb4ef46915e5 |
|---|
| 출처 메모 | uspto-grants-2013_09 |
|---|
