Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(4-Bromo-3-methylphenyl)ethanone → (R)-2-methyl-propane-2-sulfinic acid [1-(4-bromo-3-methyl-phenyl)ethylidene]-amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(4-Bromo-3-methylphenyl)ethanone | HCID 347124 | — |
| 반응물 | tert-Butylsulfinamide, (R)-(+)- | HCID 10964479 | — |
| 반응물 | 6-cyclopropyl-6-(2-hydroxy-2-methylpropyl)-3-((S)-1-(4-(1-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenyl)ethyl)-1,3-oxazinan-2-one | HCID 59635673 | — |
| 생성물 | (R)-2-methyl-propane-2-sulfinic acid [1-(4-bromo-3-methyl-phenyl)ethylidene]-amide | HCID 86649415 | — |
반응 단계
The title compound was prepared from 1-(4-bromo-3-methyl-phenyl)-ethanone and (R)-2-methyl-2-propanesulfinamide following a procedure analogous to that described in Step 1 of Intermediate 1. Mass spectrum (ESI+): m/z=316/318 (Br) [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08754076B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-0366ea9212504e35be66d107deb121e8 |
| 출처 메모 | uspto-grants-2014_06 |