Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(R)-2-methyl-propane-2-sulfinic acid [(S)-1-(4-bromo-3-methyl-phenyl)-ethyl]amide → (S)-1-(4-Bromo-3-methylphenyl)ethan-1-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (R)-2-methyl-propane-2-sulfinic acid [(S)-1-(4-bromo-3-methyl-phenyl)-ethyl]amide | HCID 58102400 | — |
| 반응물 | 6-cyclopropyl-6-(2-hydroxy-2-methylpropyl)-3-((S)-1-(4-(1-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenyl)ethyl)-1,3-oxazinan-2-one | HCID 59635673 | — |
| 생성물 | (S)-1-(4-Bromo-3-methylphenyl)ethan-1-amine | HCID 58102381 | — |
반응 단계
The title compound was prepared from (R)-2-methyl-propane-2-sulfinic acid [(S)-1-(4-bromo-3-methyl-phenyl)-ethyl]amide following a procedure analogous to that described in Step 3 of Intermediate 1. LC-MS (Method 4): tR=3.56 min; Mass spectrum (ESI+): m/z=214/216 (Br) [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08754076B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-496658468de8433b85c9577a14133e47 |
| 출처 메모 | uspto-grants-2014_06 |