Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 40922생성일: 2026년 10월 23일
3'-(Trifluoromethyl)acetophenone → (2E)-3-(dimethylamino)-1-[3-(trifluoromethyl)phenyl]prop-2-en-1-one
https://huagongshe.com/ko/reaction/40922
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3'-(Trifluoromethyl)acetophenone | HCID 67682 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | (2E)-3-(dimethylamino)-1-[3-(trifluoromethyl)phenyl]prop-2-en-1-one | HCID 5398493 | — |
반응 단계
1-[5-(Trifluoromethyl)phenyl]ethanone (0.20 mL, 0.0013 mol) and 1,1-dimethoxy-N,N-dimethylmethanamine (0.17 mL, 0.0013 mol) were combined in a sealed tube and heated in a microwave to 120° C. for 15 minutes, the reaction was allowed to cool and was concentrated to remove the residual DMF acetal, to give (2E)-3-(dimethylamino)-1-[3-(trifluoromethyl)phenyl]prop-2-en-1-one, 0.32 gm, as a red oil, LC/MS (M+H)+: 244.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08530485B2 |
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| 출처 데이터셋 | uspto-grants-2013_09 |
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| ORD ID | ord-6fbc65bb89434ec29e2e71693ea2bdfb |
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| 출처 메모 | uspto-grants-2013_09 |
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