참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | Pentafluorobenzyl bromide | HCID 74484 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | (2,3,4,5,6-Pentafluorophenyl)methyl-triphenyl-phosphonium;bromide | HCID 21282127 | — |
반응 단계
The toluene solution from Stage 1 was mixed with triphenyl phosphine (1 g) and heated at 130° C. for 3 hours. After cooling, the solution was diluted with diethyl ether (5 cm3) and the title compound filtered off, washed with hexane (4×5 cm3) and dried by suction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04791139 |
|---|
| 출처 데이터셋 | uspto-grants-1988_12 |
|---|
| ORD ID | ord-071913ea308748ad9b60322c80e9fd44 |
|---|
| 출처 메모 | uspto-grants-1988_12 |
|---|
