Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(4-Nitrophenoxy)ethanol → 2-(4-Aminophenoxy)ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(4-Nitrophenoxy)ethanol | HCID 85381 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-(4-Aminophenoxy)ethanol | HCID 80892 | 96% |
반응 단계
A suspension of 2-(4-nitrophenoxy)ethanol (Aldrich) (2 g, 10.9 mmol) and Pd/C (Aldrich, 10%, 0.2 g) in methanol (50 mL) was vigorously shaken in a Parr under atmosphere of H2 (50 psi) for 1 h. The mixture was filtered through a short pad of celite. The filtrate was concentrated to give 2-(4-amino-phenoxy)-ethanol as a light yellow solid (1.6 g, 96%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08088815B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-6f42c990a485437e913f7f2f549a027d |
| 출처 메모 | uspto-grants-2012_01 |