Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → Aluminum
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Aluminum chloride, hexahydrate | HCID 24564 | — |
| 반응물 | HCID 10233207 | HCID 10233207 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Aluminum | HCID 5359268 | — |
| 생성물 | HCID 10233207 | HCID 10233207 | — |
반응 단계
A portion of the above pure diisobutylphosphinic acid (135.01 g, 0.758 mol) was mixed with water and neutralized with dilute aqueous sodium hydroxide solution. The neutralized product was then mixed with a solution of 61.83 g (0.256 mol) AlCl3 6H2O in 2 L water. A large amount of white precipitate was observed. The precipitate was filtered and dried to a constant weight in an oven at 105° C. A white powder, aluminum salt of diisobutylphosphinic acid, of 139.43 g was obtained. The yield was 98.9%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08097747B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-d2d3394aca7145b0bec458126a88fb35 |
| 출처 메모 | uspto-grants-2012_01 |