Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sesamol → 3-(4-chloro-5-fluoro-2-hydroxyphenyl)-3-hydroxy-1-pentyl-1,3-dihydro-2H-indol-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sesamol | HCID 68289 | — |
| 반응물 | 3-Chloro-4-fluorophenol | HCID 75790 | — |
| 반응물 | 1-Pentyl-1H-indole-2,3-dione | HCID 1581092 | — |
| 반응물 | 4-bromo-1-pentyl-1H-indole-2,3-dione | HCID 28492458 | — |
| 생성물 | 3-(4-chloro-5-fluoro-2-hydroxyphenyl)-3-hydroxy-1-pentyl-1,3-dihydro-2H-indol-2-one | HCID 58872497 | — |
반응 단계
Following the procedure as described in PREPARATION 1C, and making non-critical variations to replace 4-bromo-1-pentyl-1H-indole-2,3-dione with 1-pentyl-1H-indole-2,3-dione, and 1,3-benzodioxol-5-ol with 3-chloro-4-fluorophenol, the title compound was obtained (14%): MS (ES+) m/z 346 (M−17), 386 (M+23).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08106087B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-7ea05cba03914eaa822c6655154cdf0a |
| 출처 메모 | uspto-grants-2012_01 |