Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Chloro-5-formyl-1,3-dimethyluracil → 1,3-Dimethyl-6-(methylthio)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Chloro-5-formyl-1,3-dimethyluracil | HCID 319971 | — |
| 반응물 | Sodium methanethiolate | HCID 4378561 | — |
| 생성물 | 1,3-Dimethyl-6-(methylthio)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde | HCID 86658685 | — |
반응 단계
The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.404 g, 2.00 mmol) and sodium thiomethoxide (0.154 g, 2.20 mmol in 4 ml 1,4-dioxane) were used to obtain the title compound. The crude product was purified by washing with n-pentane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536210B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-c7198cb84a3645cf8fbf9974ac7f14d0 |
| 출처 메모 | uspto-grants-2013_09 |