Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanethiol → 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanethiol | HCID 6343 | — |
| 반응물 | 6-Chloro-5-formyl-1,3-dimethyluracil | HCID 319971 | — |
| 생성물 | 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde | HCID 58484335 | — |
반응 단계
The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.303 g, 1.50 mmol) and ethanethiol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (1:1) as the eluent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536210B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-dbafb17038e6410e997a1aa39eb95162 |
| 출처 메모 | uspto-grants-2013_09 |