참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phthalic Anhydride | HCID 6811 | — |
| 반응물 | Hydroxylamine sulfate | HCID 24846 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-Hydroxyphthalimide | HCID 10665 | — |
반응 단계
0.15 g (1.0 mmol) of phthalic anhydride was mixed with 0.2 to 1 equivalent of hydroxylammonium sulfate (see Table 1) and, optionally after the addition of water (see Table 1), heated to 130° C. in a sealed ampoule. The reaction times were varied for the individual mixtures in accordance with Table 1. The cooled reaction mixture was dissolved in d6-DMSO and analyzed using 1H-NMR spectroscopy. The yields are given in each case in Table 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06316639B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_11 |
|---|
| ORD ID | ord-e3ee272c6b29480f9ca62db9970c86f7 |
|---|
| 출처 메모 | uspto-grants-2001_11 |
|---|
