Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclopropaneacetic acid → N-(Cyclopropylacetyl)-L-alanine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclopropaneacetic acid | HCID 138440 | — |
| 반응물 | Alanine methyl ester hydrochloride | HCID 2733257 | — |
| 생성물 | N-(Cyclopropylacetyl)-L-alanine | HCID 54556694 | — |
반응 단계
Following General Procedure A above using cyclopropylacetic acid (Aldrich) and L-alanine methyl ester hydrochloride (Sigma), the title compound was prepared as an oil. The reaction was monitored by tic on silica gel (Rf=0.15 in 25% ethyl acetate/hexanes) and purification was by flash column chromatography using 25% ethyl acetate/hexanes as the eluant.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06667305B1 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-d53239e2e6b748a1ba0c280bac48c371 |
| 출처 메모 | uspto-grants-2003_12 |