Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 6-Methoxy-2-naphthylacetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | Methyl 6-methoxynaphthalene-2-acetate | HCID 90324 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 6-Methoxy-2-naphthylacetic acid | HCID 32176 | — |
반응 단계
A mixture of 25 g. of methyl 6-methoxy-2-naphthylacetate, 15 g. of sodium carbonate, 200 ml. of methanol, and 25 ml. of water are stirred for 24 hours. The reaction mixture is then acidified with 200 ml. of 2 N hydrochloric acid and extracted with methylene chloride. The extracts are combined, washed with water, dried over sodium sulfate, and evaporated to yield 6-methoxy-2-naphthylacetic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04009197 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-3b933a6a881645fa95e6a20e77521c65 |
| 출처 메모 | uspto-grants-1977_02 |