Water → 1-(Hydroxymethyl)cyclohexan-1-ol

HRID 442049

반응식

HRID 442049 반응식
N[CH2:2][C:3]1([OH:9])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[OH2:10]>>[OH:10][CH2:2][C:3]1([OH:9])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1

참가 물질

3

반응물 2

HCID 962WaterHCID 776141-(Aminomethyl)cyclohexan-1-ol

생성물 1

HCID 2512591-(Hydroxymethyl)cyclohexan-1-ol

실험 절차

Compounds of this type may be prepared from isophorone utilizing the methods described in U.S. Pat. Nos. 3,270,044 and 3,352,913 to form an amino methyl cyclohexanol which is then reacted with a carboxylic acid in a fusion cook by heating stoichiometric quantities of the amine and the acid until molten and stirring the molten mixture with a nitrogen sweep to drive off water vapor. The progress of the reaction is stopped when an acid number just below theoretical is obtained. Similarly, the carboxylate derivative can be formed from a hydroxymethyl cyclohexanol.

후처리

  1. custombelow theoretical is obtained

출처 및 근거

ORD 기록
ord-bdd398d5c3704a7b95a78d2539cfe0b5
출처 데이터셋
uspto-grants-1977_08
특허 번호
US04044033

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