Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bisphenol A → 1,1,3,3-Tetramethylindan-5-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bisphenol A | HCID 6623 | — |
| 반응물 | 4-tert-Butylphenol | HCID 7393 | — |
| 생성물 | 1,1,3,3-Tetramethylindan-5-ol | HCID 104567 | — |
반응 단계
172.5 g (1.15 mol) of 4-tert.-butylphenol, 57.5 g (0.25 mol) of 2,2-bis-(4-hydroxyphenyl)-propane and 10 g of an acid-activated fuller's earth were heated with stirring in an autoclave for 6 hours to approximately 200° C. The hot reaction mixture is then filtered off from the catalyst under suction and the resulting 221.3 g reaction mixture subjected to fractional distillation in vacuo, giving 25.2 g (52 % of the theoretical) of 5-hydroxy-1,1,3,3-tetramethyl indane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04045499 |
| 출처 데이터셋 | uspto-grants-1977_08 |
| ORD ID | ord-34f10486ae7a4d51b76d8f62fa67a75a |
| 출처 메모 | uspto-grants-1977_08 |