Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 9H-thioxanthen-9-ol | HCID 5154170 | — |
| 반응물 | Ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate Ethyl-4-cyanobenzoyl acetate | HCID 131721214 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate | HCID 54398664 | — |
반응 단계
Ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate Ethyl-4-cyanobenzoyl acetate (6 g, 28 mmol) and 9-hydroxy thioxanthene (6.6 g, 31 mmol) were mixed in acetic acid (50 ml) and ethanol (50 ml) using the procedure described in Example 3 (ii) to give ethyl 2-(4-cyanobenzoyl)-2-(9H-thioxanthen-9-yl)acetate as a pale yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05891899 |
| 출처 데이터셋 | uspto-grants-1999_04 |
| ORD ID | ord-200afce35b8c4cbdbd597f47e8853533 |
| 출처 메모 | uspto-grants-1999_04 |