Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenyl phenylglyoxylate → Phenyl 4-chlorobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenyl phenylglyoxylate | HCID 13975017 | — |
| 반응물 | 4-Chlorophenyl phenylglyoxylate | HCID 54442020 | — |
| 촉매 | Tetraphenylphosphonium Chloride | HCID 164911 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Phenyl 4-chlorobenzoate | HCID 260766 | — |
반응 단계
The decarbonylation reaction of Example 79 was repeated except that phenyl phenylglyoxylate (PPG) was replaced with 4-chlorophenyl phenylglyoxylate (4-CPPG), and that the amounts of tetraphenylphosphonium chloride and chloroform were changed as set forth in Table 13. The results are set forth in Table 13.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05892091 |
| 출처 데이터셋 | uspto-grants-1999_04 |
| ORD ID | ord-b4c01714edc043b29f69990524dc94d0 |
| 출처 메모 | uspto-grants-1999_04 |