Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
O-Methylhydroxylamine → 2-(Methoxyamino)quinazolin-4-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | O-Methylhydroxylamine | HCID 4113 | — |
| 반응물 | 2-Chloroquinazolin-4-amine | HCID 252879 | — |
| 생성물 | 2-(Methoxyamino)quinazolin-4-amine | HCID 57456921 | — |
반응 단계
Prepared as in Example 42 from 2-chloroquinazolin-4-amine (Example 38) and methoxylamine. 1H NMR (400 MHz, DMSO-d6) δ3.79 (s, 3H), 7.48-7.44 (m, 1H), 7.86-7.80 (m, 2H), 8.27 (d, J=8.0 Hz, 1H), 8.99 (s, 1H), 9.16 (s, 1H), 12.39-12.08 (m, 1H). MS 191 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08541421B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-0159be6d9c5b4e1189b29725576be9e0 |
| 출처 메모 | uspto-grants-2013_09 |