Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methylpiperazine → Methyl 2-(4-methylpiperazino)-5-nitrobenzenecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methylpiperazine | HCID 53167 | — |
| 반응물 | Methyl 2-Fluoro-5-nitrobenzoate | HCID 11217860 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 2-(4-methylpiperazino)-5-nitrobenzenecarboxylate | HCID 36405266 | — |
반응 단계
A solution of methyl 2-fluoro-5-nitro-benzoate (3.487 g, 17.511 mmol) and N-methylpiperazine (3.855 mL, 3.508 g, 35.022 mmol) in 30 mL of anhydrous methanol was heated to reflux for 5 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08541429B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-36509e16039c4f43b53665e1858e6db9 |
| 출처 메모 | uspto-grants-2013_09 |