Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
[1-(4-fluoro-phenyl)-2-methyl-1H-imidazol-4-yl]-methanol → 1-(4-fluoro-phenyl)-2-methyl-1H-imidazole-4-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | [1-(4-fluoro-phenyl)-2-methyl-1H-imidazol-4-yl]-methanol | HCID 67303957 | — |
| 촉매 | Manganese | HCID 23930 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1-(4-fluoro-phenyl)-2-methyl-1H-imidazole-4-carbaldehyde | HCID 85997993 | — |
반응 단계
[1-(4-Fluoro-phenyl)-2-methyl-1H-imidazol-4-yl]-methanol is dissolved in methylene chloride. Mangan (IV) oxide is added and the reaction mixture is stirred at room temperature for 3 days. The suspension is filtered through a dicalite speed plus pad and the desired compound (4-fluoro-phenyl)-2-methyl-1H-imidazole-4-carbaldehyde is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08481548B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-687063cbc1674a448e4a228f4346c316 |
| 출처 메모 | uspto-grants-2013_07 |