Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → 2-p-Cyanophenyl-5-n-pentyl-4-methyl-1,3-dioxane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | 4-Cyanobenzaldehyde | HCID 66042 | — |
| 반응물 | 3-Hydroxymethyl-2-octanol | HCID 13526101 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 2-p-Cyanophenyl-5-n-pentyl-4-methyl-1,3-dioxane | HCID 20150974 | — |
반응 단계
A mixture of 0.1 mol of p-cyanobenzaldehyde, 0.1 mol of 3-hydroxymethyl-2-octanol, 200 ml of benzene and 150 mg of p-toluenesulfonic acid is boiled under a water separator until the reaction is complete. Usual working-up gives 2-p-cyanophenyl-5-n-pentyl-4-methyl-1,3-dioxane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04726911 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-f338593bb42141e5a94468c5d011ca54 |
| 출처 메모 | uspto-grants-1988_02 |