Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl pyridine-3,5-dicarboxylate → Dimethyl piperidine-3,5-dicarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl pyridine-3,5-dicarboxylate | HCID 78339 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Dimethyl piperidine-3,5-dicarboxylate | HCID 49761012 | — |
반응 단계
Pyridine-3,5-dicarboxylic acid dimethyl ester (5.3 g, 27 mmol) and Rh/PtO2 (0.5 g) in MeOH (200 mL) are stirred under hydrogen overnight. The resulting mixture is filtered and the solvents are evaporated to give a brown oil. MS (LC-MS): 202 [M+H]+
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08497286B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-080a5bb57e19404f996977073d5869eb |
| 출처 메모 | uspto-grants-2013_07 |