Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → Methyl 3-(methylamino)but-2-enoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | Methyl acetoacetate | HCID 7757 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 3-(methylamino)but-2-enoate | HCID 2734182 | — |
반응 단계
To a solution of methyl acetoacetate (29.4 g, 253 mmol) in MeOH (30 mL) was added methylamine (33 wt % in EtOH; 48 mL, 385 mmol) dropwise at room temperature. The reaction was stirred for 1 hour, and then concentrated and dried to give the title compound as a white crystalline solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08541587B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-83d244af03f643cea719dec0d8bec63e |
| 출처 메모 | uspto-grants-2013_09 |