Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Cyclohexadiene → 5,6-Di(benzenesulfonyl)bicyclo[2.2.2]oct-2-ene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Cyclohexadiene | HCID 11605 | — |
| 반응물 | trans-1,2-Bis(phenylsulfonyl)ethylene | HCID 5367099 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 5,6-Di(benzenesulfonyl)bicyclo[2.2.2]oct-2-ene | HCID 12778411 | 96.5% |
반응 단계
29.33 g of trans-1,2-diphenylsulfonylethylene was dissolved in 200 ml of toluene, and then, 11.4 ml of 1,3-cyclohexadiene was added, followed by dry distillation for 21 hours and then by recrystallization to obtain 35.66 g (yield: 96.5%) of 5,6-diphenylsulfonyl-bicyclo-[2,2,2]oct-2-ene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07193237B2 |
| 출처 데이터셋 | uspto-grants-2007_03 |
| ORD ID | ord-a06b7c538b6d48bcb165f87e5c36eb9b |
| 출처 메모 | uspto-grants-2007_03 |