Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Borohydride → 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Borohydride | HCID 28123 | — |
| 반응물 | 6,4'-Dimethoxybiphenyl-3-carbaldehyde | HCID 22391191 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol | HCID 68841639 | 87.2% |
반응 단계
A solution of 4-methoxy-3-(4-methoxyphenyl)benzenecarboxaldehyde (1 g, 4.13 mmol) in methanol (12 mL) was treated with polymer-supported borohydride (10.3 mmol) and the mixture shaken for 16 hours. The resin was then filtered and the filtrate concentrated under reduced pressure to afford 0.88 g of title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07196102B2 |
| 출처 데이터셋 | uspto-grants-2007_03 |
| ORD ID | ord-a9f128eb66ba4a03a994df7c3c66eb4c |
| 출처 메모 | uspto-grants-2007_03 |