Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 5-(tert-Butyl)-3-chloro-4-hydroxybenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Chlorine | HCID 24526 | — |
| 반응물 | 3-(tert-Butyl)-4-hydroxybenzaldehyde | HCID 3017618 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 5-(tert-Butyl)-3-chloro-4-hydroxybenzaldehyde | HCID 3017619 | — |
반응 단계
Chlorine gas was passed into a solution of 3-tert-butyl-4-hydroxybenzaldehyde (2.5 gm) in acetic acid (20 ml) for 1 hour. The solution was poured into water and the product collected. Recrystallisation from aqueous ethanol gave 3-tert-butyl-5-chloro-4-hydroxybenzaldehyde m.p. 123° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04064266 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-35231d5d4e214396a1b80ff85b230e62 |
| 출처 메모 | uspto-grants-1977_12 |