Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → Tampramine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | [2-[(3-Amino-2-pyridinyl)[3-(dimethylamino)propyl]amino]phenyl]phenylmethanone | HCID 53769600 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Tampramine | HCID 54961 | — |
반응 단계
[2-[[3-(Dimethylamino)propyl](3-amino-2-pyridinyl)amino]phenyl]phenylmethanone from Example 21a is refluxed in excess acetic acid or in toluene solution containing a catalytic amount of p-toluene sulfonic acid to give a solution of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04518603 |
| 출처 데이터셋 | uspto-grants-1985_05 |
| ORD ID | ord-e98347ba6d34436bae05b0ae107a8077 |
| 출처 메모 | uspto-grants-1985_05 |