Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Alcohol → HCID 178476834, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Alcohol | HCID 244 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | HCID 178476830 | HCID 178476830 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | HCID 178476834 | HCID 178476834 | 91.2% |
반응 단계
A solution of α-hydroxyethylphosphinic acid (5.5 g) and benzyl alcohol (2.26 g) in benzene (50 ml) was heated for 8 hours with removal of water through a Dean-Stark apparatus. After cooling, the reaction mixture was washed with water, dried over magnesium sulfate and concentrated in vacuo to give 3.65 g (91.2%) of benzyl α-hydroxyethylphosphinate (Compound No. 36).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04544652 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-3b10e5d9b7a94dba8dfc894d8aea4436 |
| 출처 메모 | uspto-grants-1985_10 |