Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiophenol → N-benzyloxycarbonyl-glycine-phenythio ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiophenol | HCID 7969 | — |
| 반응물 | Benzyloxycarbonylglycine | HCID 14349 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-benzyloxycarbonyl-glycine-phenythio ester | HCID 22764889 | 62% |
반응 단계
Using thiophenol and Z-Gly.OH, Example 78 was repeated; except that dichloromethane was used in place of ethyl acetate as the extraction solvent, to obtain N-benzyloxycarbonyl-glycine-phenythio ester (hereinafter represented by ##STR12## in a yield of 62%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04173563 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-01bd8ea14e7b4957854705e522f04f34 |
| 출처 메모 | uspto-grants-1979_11 |