Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 3-Phenyl-1-indanone oxime
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-Indanone, 3-phenyl- | HCID 98146 | — |
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 3-Phenyl-1-indanone oxime | HCID 73183939 | — |
반응 단계
A mixture of 3-phenylindan-1-one (80 g), methanol (935 ml), water (90 ml), potassium carbonate (103.8 g), and hydroxylamine HCl (104.3 g) was heated at reflux for 16 hours, then poured into ice-water: the title compound was filtered, washed with water, with a small portion of ether, then dried in air. Yield: 74.7 g; m.p. 133°-139°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04548946 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-06804961a4a94f6fab538831a07fec43 |
| 출처 메모 | uspto-grants-1985_10 |