Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dinitrofluorobenzene → 1-(2-Acetamidoethyl)-5-(2,4-dinitrophenylthio)tetrazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dinitrofluorobenzene | HCID 6264 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | HCID 178474869 | HCID 178474869 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-(2-Acetamidoethyl)-5-(2,4-dinitrophenylthio)tetrazole | HCID 20382814 | — |
반응 단계
A solution of 9.3 g. (0.050 mol) of 2,4-dinitrofluorobenzene in 50 ml. of acetone was added to a solution of 9.35 g. (0.050 mol) of 1-(2-acetamidoethyl)tetrazole-5-thiol and 6.85 ml. (0.050 mol) of triethylamine in 100 ml. of acetone and the reaction mixture was stirred for 1 hour. The solid material was collected by filtration and recrystallized from acetonitrile to give 1-(2-acetamidoethyl)-5-(2,4-dinitrophenylthio)tetrazole, mp 197°-198° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04174323 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-937d28167899414e8b05586171b8ea76 |
| 출처 메모 | uspto-grants-1979_11 |