Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexanoic Acid → 7-Methyl-2-pentyl-3H-imidazo[4,5-b]pyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexanoic Acid | HCID 8892 | — |
| 반응물 | 4-Methylpyridine-2,3-diamine | HCID 317495 | — |
| 생성물 | 7-Methyl-2-pentyl-3H-imidazo[4,5-b]pyridine | HCID 19814121 | — |
반응 단계
The title compound was prepared from 2,3-diamino-4-picoline (0.246 g, 2 mmol) and hexanoic acid (0.25 ml, 2 mmols) according to the procedure described in Step 1 of Example 9. The crude product was purified by flash chromatography on silica-gel using EtOAc-MeOH (9:1) to give the pure product (0.28 g, 69%) as a tan colored solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05157026 |
| 출처 데이터셋 | uspto-grants-1992_10 |
| ORD ID | ord-841ec3cba52e428982d1c07469bac46d |
| 출처 메모 | uspto-grants-1992_10 |