Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Epiandrosterone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 3beta-Acetoxy-5alpha-androstan-17-one | HCID 908740 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Epiandrosterone | HCID 441302 | 95% |
반응 단계
A mixture of 5 (1 g, 3.00 mmol), NaOH 0.12 g (3.44 mmol) in methanol was refluxed for 10 min, cooled to room temperature and treated with water. The resulting precipitate was filtered off and washed with water to afford crude product 6 (0.82 g, 95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08623849B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-ae5f46f7bef043fb87e21b3a77341060 |
| 출처 메모 | uspto-grants-2014_01 |