Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(4-amino-2-butyl-1H-imidazo[4,5-c][1,5]naphthyridin-1-yl)ethaneamine → HCID 178441566, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(4-amino-2-butyl-1H-imidazo[4,5-c][1,5]naphthyridin-1-yl)ethaneamine | HCID 21946027 | — |
| 반응물 | HCID 178524392 | HCID 178524392 | — |
| 생성물 | HCID 178441566 | HCID 178441566 | 21.8% |
반응 단계
Using the general method of Example 97 6-hydroxypicolinic acid (0.24 g, 1.7 mmole) was reacted with 2-(4-amino-2-butyl-1H-imidazo[4,5-c][1,5]naphthyridin-1-yl)ethaneamine (0.5 g, 1.7 mmol) to provide 0.15 g of N-[2-(4-amino-2-butyl-1H-imidazo[4,5-c][1,5]naphthyridin-1-yl)ethyl]-6-hydroxy-2-pyridinecarboxamide as a white powder, m.p. 258-260° C. Analysis: Calculated for C21H23N7O2+½ CH3CN: %C, 62.03; %H, 5.80; %N, 24.66. Found: %C, 61.87; %H, 5.70; %N, 24.60.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06699878B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-e9083d2ce62d487684022ded273cd3d7 |
| 출처 메모 | uspto-grants-2004_03 |