Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 3beta-Acetoxyandrost-5-en-17-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Dehydroepiandrosterone | HCID 5881 | — |
| 생성물 | 3beta-Acetoxyandrost-5-en-17-one | HCID 14709 | — |
반응 단계
Dehydroepiandrosterone (2.88 g, 10 mmol) is dissolved in a mixture (100 ml) of anhydride acetic and pyridine (1:1 v/v) and left at room temperature for 16 h. The mixture is then poured carefully into iced water and after 16 h, crystals are filtered and dried in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05798347 |
| 출처 데이터셋 | uspto-grants-1998_08 |
| ORD ID | ord-f366acb5aafd4c8cbb8b947328ca6470 |
| 출처 메모 | uspto-grants-1998_08 |