Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methyl-2-piperidinemethanol → N-methyl-2-piperidylmethyl N,N-dimethylaminoacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methyl-2-piperidinemethanol | HCID 89394 | — |
| 반응물 | Glycine, N,N-dimethyl-, ethyl ester | HCID 118412 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-methyl-2-piperidylmethyl N,N-dimethylaminoacetate | HCID 19753089 | — |
반응 단계
A mixture of 75 g of ethyl N,N-dimethylglycinate, 75 g of 1-methyl-2-piperidylmethanol and 1 g of titanium tetra(n-butoxide) was heated at 45° C. until the amount of ethanol collected indicated the reaction was complete. After cooling a small amount of water was added, the mixture was filtered, and the filtrate was distilled under reduced pressure to provide N-methyl-2-piperidylmethyl N,N-dimethylaminoacetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05225513 |
| 출처 데이터셋 | uspto-grants-1993_07 |
| ORD ID | ord-d6308de8a1ec43cdb67084bf42d56e20 |
| 출처 메모 | uspto-grants-1993_07 |