Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Arecoline → 3-Methoxycarbonyl-1-methyl-4-(3-trifluoromethylphenyl)piperidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Arecoline | HCID 2230 | — |
| 반응물 | Benzene, 1-bromo-3-(trifluoromethyl)- | HCID 9817 | — |
| 생성물 | 3-Methoxycarbonyl-1-methyl-4-(3-trifluoromethylphenyl)piperidine | HCID 19751261 | — |
반응 단계
3-methoxycarbonyl-1-methyl-4-(3-trifluoromethylphenyl)piperidine was prepared as the cis/trans mixture from arecoline and 3-bromo-trifluoromethylbenzene as described (J. Org. Chem. 22 (1957) 261). The product was purified by vacuum distillation. B.p. 90°-110° C./0.7 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05227379 |
| 출처 데이터셋 | uspto-grants-1993_07 |
| ORD ID | ord-1a232e0c4acd4c8195c3f74b996ba32d |
| 출처 메모 | uspto-grants-1993_07 |