Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → p-Tetradecyloxyphenylacetylchloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | p-Tetradecyloxyphenylacetic acid | HCID 10472964 | — |
| 촉매 | Dimethylformamide | HCID 6228 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | p-Tetradecyloxyphenylacetylchloride | HCID 10021844 | 97.6% |
반응 단계
A mixture of 21.7 g of p-tetradecyloxyphenylacetic acid and 11.85 g of oxalyl chloride, 45.5 mg of N,N-dimethylformamide and 250 ml of methylene chloride is stirred at ambient temperature for 24 hours. The solvent is removed by evaporation and the residue is dissolved in ether and filtered through diatomaceous earth. The filtrate is evaporated to give 22.3 g of the desired product as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05231182 |
| 출처 데이터셋 | uspto-grants-1993_07 |
| ORD ID | ord-10bd3f37a79a403ab89d4b746b343574 |
| 출처 메모 | uspto-grants-1993_07 |