Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbon Dioxide → Ethyl 2-bromo-3-phenylpropanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbon Dioxide | HCID 280 | — |
| 반응물 | Ethyl bromo-(phenylmethyl)propanedioate | HCID 86007639 | — |
| 생성물 | Ethyl 2-bromo-3-phenylpropanoate | HCID 4737529 | — |
반응 단계
Ethyl bromo-(phenylmethyl)propandioate (XXVI, Example 60, 130 g.) is heated under reduced pressure to 140° with vigorous evolution of carbon dioxide. When decarboxylation is complete (about 5 minutes), the mixture is distilled to give ethyl 2-bromo-3-phenylpropionate, b.p. 120°/30 mm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04534897 |
| 출처 데이터셋 | uspto-grants-1985_08 |
| ORD ID | ord-105355d6d3dc4bf48e8128d58f3d322d |
| 출처 메모 | uspto-grants-1985_08 |