Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Methyl 9-hydroxy-9H-fluorene-9-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Flurenol | HCID 10087 | — |
| 생성물 | Methyl 9-hydroxy-9H-fluorene-9-carboxylate | HCID 267210 | — |
반응 단계
9-Hydroxy-9H-fluorene-9-carboxylic acid (Aldrich Chemical, Inc.) (20.0 g, 88.4 mmol) was added to 100 mL methanol saturated with hydrogen chloride and mixture was stirred at reflux for 4 h. The crystalline material obtained on cooling was collected by filtration and washed with cold 1:1 ethyl acetate/hexane to provide after drying (1), 15.8 g (74%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04537892 |
| 출처 데이터셋 | uspto-grants-1985_08 |
| ORD ID | ord-9ffad41ed7b441e793e76f32ace11b60 |
| 출처 메모 | uspto-grants-1985_08 |