Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene, 1-chloro-3-isocyanato- → 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene, 1-chloro-3-isocyanato- | HCID 17968 | — |
| 반응물 | N-nitroimidazolidin-2-imine | HCID 135413413 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine | HCID 136342791 | — |
반응 단계
A solution of 3.9 g of 2-nitroiminoimidazolidine and 4.6 g of 3-chlorophenylisocyanate in 80 ml of dry acetonitrile was refluxed for 3 hours. After cooling to room temperature, the precipitated crystals were filtered, and washed with ether to give desired 1-(3-chlorophenylcarbamoyl)-2-nitroiminoimidazolidine. The yield was 4.7 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05298507 |
| 출처 데이터셋 | uspto-grants-1994_03 |
| ORD ID | ord-28cb280ddd404d7ead70255ca3b81e8e |
| 출처 메모 | uspto-grants-1994_03 |