Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(2-Bromophenyl)-1,3-dioxolane → Methyl 2-(1,3-dioxolan-2-yl)-phenylglyoxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(2-Bromophenyl)-1,3-dioxolane | HCID 553534 | — |
| 반응물 | Oxalic acid monomethyl ester chloride | HCID 86640482 | — |
| 촉매 | Zinc | HCID 23994 | — |
| 생성물 | Methyl 2-(1,3-dioxolan-2-yl)-phenylglyoxylate | HCID 21752929 | — |
반응 단계
174.5 g of 1-bromo-2-(1,3-dioxolan-2-yl)-benzene was reacted via the zinc-organic compound with 102 g of oxalic acid monomethyl ester chloride, analogously to Example 2. Yield: 41.6 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05298527 |
| 출처 데이터셋 | uspto-grants-1994_03 |
| ORD ID | ord-6b1cc3f93a7743eb8a865a217795b220 |
| 출처 메모 | uspto-grants-1994_03 |