Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Hydrochloric Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide | HCID 22293288 | — |
| 생성물 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 3-Azido-5-fluoropyridin-2-amine | HCID 22293242 | — |
반응 단계
N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide (275 mg, 1.16 mmol) in 3 N HCl (5 mL) was heated to 100° C. After 2 h, the volatiles were removed in vacuo, to give the title compound as its HCl salt (180 mg). MS 154.2 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07534784B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-f4250e275695472dbc2393a5e31a0711 |
| 출처 메모 | uspto-grants-2009_05 |