Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 4-Carboxyphenylboronic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Tolylboronic acid | HCID 79799 | — |
| 반응물 | Potassium Permanganate | HCID 516875 | — |
| 생성물 | 4-Carboxyphenylboronic Acid | HCID 312183 | — |
반응 단계
To a solution of 4-methylphenylboronic acid (34 g, 0.25 mol) in aqueous sodium hydroxide (0.5 N, 1000 mL) was added potassium permanganate (83 g, 0.53 mol) while keeping the temperature at 35-40° C. After the addition the reaction was filtered and the filtrate acidified with concentrated hydrochloric acid (65 mL). The product was filtered off. A yield of 29.6 g was obtained. M.p. 228° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06706749B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-85361952dc384526833644ea8fd303a8 |
| 출처 메모 | uspto-grants-2004_03 |