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HRID 494435생성일: 2026년 10월 24일

Methyl 2-allyl-2-phenyl-4-pentenoate → Methyl 2-phenyl-2-propylpentanoate

https://huagongshe.com/ko/reaction/494435

반응식

참여 물질

역할이름HCID투입량
반응물Methyl 2-allyl-2-phenyl-4-pentenoateHCID 11085592—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물Methyl 2-phenyl-2-propylpentanoateHCID 11658708100%

반응 조건

온도25 °C

반응 단계

A solution of the product of Example 1A (7.5 g, 32.61 mmol) in ethyl acetate (125 mL) was treated with 10% palladium on carbon (600 mg) and stirred at 25° C. under hydrogen gas for 18 hours. The solution was filtered through Celite® and the filtrate was concentrated in vacuo to give the title compound (7.63 g, 100%). 1H NMR (300 MHz, CDCl3): δ 7.27 (m, 5 H), 3.64 (m, 3 H), 1.96 (m, 4 H), 1.08 (m, 4 H), 0.89 (t, J=7.17 Hz, 6 H).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07538105B2
출처 데이터셋uspto-grants-2009_05
ORD IDord-2e16aba769f441d2b0e0d965dd200900
출처 메모uspto-grants-2009_05