Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Benzyloxy)-6-butylpyridine → 6-Butylpyridin-2-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Benzyloxy)-6-butylpyridine | HCID 66626481 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 6-Butylpyridin-2-ol | HCID 23352100 | — |
반응 단계
To a pressure reaction bottle were added 1.6 g 2-(benzyloxy)-6-butylpyridine, 0.2 g 5% palladium on carbon and 50 ml ethanol. The mixture was hydrogenated at 22 C and 40 psi hydrogen for 16 hours. Following filtration through celite and solvent removal, an oil was obtained that crystallized on standing to give 0.9 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07538931B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-9846a64eb1374f1db7869785d1743f74 |
| 출처 메모 | uspto-grants-2009_05 |