Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → 4-(Naphth-1-yl)piperidine hydrobromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | Ethyl [4-(naphth-1-yl)piperid-1-yl]carbamate | HCID 54406105 | — |
| 생성물 | 4-(Naphth-1-yl)piperidine hydrobromide | HCID 19096220 | 86.64% |
반응 단계
10.5 g of the compound obtained in Stage A in 300 ml of a 48% hydrobromic acid solution, are refluxed for 20 hours. After evaporation and washing twice with ethanol, the residue is taken up in acetone and the mixture then filtered to give 4-(naphth-1-yl)piperidine hydrobromide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05242933 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-2b73ef6cf0d74456b104b1399812863b |
| 출처 메모 | uspto-grants-1993_09 |