Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Decanoate → Decanohydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Decanoate | HCID 8050 | — |
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Decanohydrazide | HCID 98597 | 94% |
반응 단계
17.5 g of decanoic acid methyl ester is dissolved in 1 l of absolute ethanol and mixed with 350 ml of hydrazine hydrate. It is refluxed for 3 hours and then stirred overnight at room temperature. The solution is concentrated by evaporation to about 300 ml and allowed to stand until the product is crystallized out. After it is filtered off and dried, 16.6 g (=94% of theory) of decanoic acid hydrazide is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06709693B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-d63e462b8fd14c8bbc6a3c4b6aae5b72 |
| 출처 메모 | uspto-grants-2004_03 |